0.  SQUALOR PRELIMINARY EXAMINATION



Name of Chemist-1: _____________________________                         	





SQUALOR Unknown Number:







SQUALOR Unknown Number:









Name of unknown:







Name of unknown:









Bond line drawing of unknown:











Bond line drawing of unknown:















Name of Chemist-2: _____________________________                         	





SQUALOR Unknown Number:







SQUALOR Unknown Number:









Name of unknown:







Name of unknown:









Bond line drawing of unknown:











Bond line drawing of unknown:
















THE REMAINDER OF THIS REPORT IS FOR YOUR ACTUAL UNKNOWN, NOT SQUALOR!


Unknown Number: _______


I.  PHYSICAL PROPERTIES

A.  Melting/Boiling point:  __________


B.  Solubility Characteristics (Circle each that applies):


1.  Water           +      -

2.  1M HCl          +      -      n/a

3.  1M NaOH         +      -      n/a

4.  NaHCO3          +      -      n/a

5.  H2SO4            +      -      n/a


Conclusions based upon solubility only:






II.  SPECTRAL PROPERTIES

Attach infrared spectrum of the unknown with this report.  Note the presence (or
absence) of any spectral bands that helped you to determine the identity of your
unknown:
















III.  CLASSIFICATION TESTING

For each of the following that apply, indicate whether you obtained a positive or
negative result for your unknown.  If you did not perform the test, simply circle
n/a.


A.  Chromic Acid test           +      -      n/a

B.  Ferric Chloride test        +      -      n/a

C.  Iodoform test               +      -      n/a

D.  2,4-DNPH test               +      -      n/a

E.  Baeyer test                 +      -      n/a

F.  Br2 in CCl4                 +      -      n/a

G.  Miscellaneous tests not listed above:  list name of test, source of the test
and result.










Comment on the results of the classification tests.  What have they told you?








IV.  DERIVATIZATION

For each derivative which you formed, write a chemical reaction showing the
starting materials and the products formed.  Also list the melting point of the
derivative and the melting point found in the table in the text for that
derivative.

A.  Derivative 1

1. Reaction:










2. Melting point:  _______

3. Table value:    _______


B.  Derivative 2

1. Reaction:









2. Melting point:  _______

3. Table value:    _______

V.  THE FINALE

DRAW YOUR UNKNOWN AND GIVE ITS NAME: